Nano-Silica phosphoric acid: an efficient catalyst for one-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones (thiones) under solvent-free or sonication conditions

نویسندگان

  • Abdolhamid Bamoniri Department of Organic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, I.R.Iran.
  • Bi Bi Fatemeh Mirjalili Department of Chemistry, College of Science, Yazd University, I. R. Iran .
  • Sedigheh Nazemian Department of Chemistry, College of Science, Yazd University, I. R. Iran .
چکیده مقاله:

Two simple protocols for the synthesis of three-component condensation reaction of an aldehyde, β-ketoester and urea or thiourea to obtain the 3, 4-dihydropyrimidin-2(1H)-ones (thiones) using nano silica phosphoric acid are reported. Short reaction times, high yields, reusability of catalyst and easy workup are some advantages of these protocols.

منابع مشابه

nano-silica phosphoric acid: an efficient catalyst for one-pot synthesis of 3,4-dihydropyrimidin-2(1h)-ones (thiones) under solvent-free or sonication conditions

two simple protocols for the synthesis of three-component condensation reaction of an aldehyde, β-ketoester and urea or thiourea to obtain the 3, 4-dihydropyrimidin-2(1h)-ones (thiones) using nano silica phosphoric acid are reported. short reaction times, high yields, reusability of catalyst and easy workup are some advantages of these protocols.

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Two simple protocols for the synthesis of tetrahydrobenzo[a]xanthenes-11-ones using nano silica phosphoric acid are reported. Short reaction times, high yields, reusability of catalyst and easy workup are some advantages of these protocols.

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nano-silica phosphoric acid: an efficient catalyst for one-pot synthesis of tetrahydrobenzo[a]xanthenes-11-one under solvent- free or sonication conditions

two simple protocols for the synthesis of tetrahydrobenzo[a]xanthenes-11-ones using nano silica phosphoric acid are reported. short reaction times, high yields, reusability of catalyst and easy workup are some advantages of these protocols.

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4-Sulfobenzoic Acid as an Efficient Catalyst for the Preparation of 3,4-dihydropyrimidin-2-(1H)-ones Under Solvent-free Conditions

In this research, one-pot three-component synthesis of 3,4-dihydropyrimidin-2-(1H)-ones havebeen developed using Biginelli reaction from the interaction between ethyl/methyl acetoacetate,aromatic aldehydes, and urea/thiourea in the presence of 4-sulfobenzoic acid as a new, effective,inexpensive, and available bronsted acid. Avoidance of toxic and dangerous solvents, easy isola...

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Nano Silica Phosphoric Acid: An Efficient Catalyst for the One- Pot Synthesis of 1, 2, 4, 5-Tetrasubstituted Imidazoles

Two  simple  protocols  for  the  synthesis  of  1,  2,  4,  5-   tetrasubstitutedimidazoles  using  nano-SPA  as  a  reusable,  eco-   friendly,  inexpensive,  and  efficient  catalyst  are  reported.  Short   reaction  times,  high  yields,  scale-up  and  easy  workup  are  the   advantages of these protocols.

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عنوان ژورنال

دوره 2  شماره 1

صفحات  17- 21

تاریخ انتشار 2012-01-01

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